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Foodstuffs. Determination of ochratoxin A in spices, liquorice, cocoa and cocoa products by IAC clean-up and HPLC-FLD Ingestion-build-51215 What is BS 2782-3: Method1 Scope This document specifies a procedure for the determination of ochratoxin A (OTA) in chilli, paprika, black and white pepper, nutmeg, spice mix, liquorice (root and extracts), cocoa and cocoa products by high performance liquid chromatography (HPLC) with immunoaffinity column clean up and fluorescence detection (FLD). This method has been validated in interlaboratory studies via the analysis of both naturally contaminated and spiked samples